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Quantitative mechanical characterization of materials at the nanoscale through direct measurement of time-resolved tip–sample interaction forces

M Balantekin et al 2008 Nanotechnology 19 085704 (6pp)   doi: 10.1088/0957-4484/19/8/085704  Help

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M Balantekin, A G Onaran and F L Degertekin
The George W Woodruff School of Mechanical Engineering, Georgia Institute of Technology, Atlanta, GA 30332-0405, USA
E-mail: mujdat@gatech.edu

Abstract. We introduce a new method for material characterization at the nanoscale using a recently developed atomic force microscope (AFM) probe. The FIRAT (force sensing integrated readout and active tip) probe is integrated into a commercial AFM system to obtain time-resolved interaction forces (TRIFs) between the probe tip and sample at speeds suitable for nondestructive and fast imaging of material properties. We present a basic interaction model to extract the material elasticity and surface energy. Numerical simulations are performed and compared to the experimental results for three different polymers and a silicon sample. We find that our interaction model does not completely explain the observed long-range surface forces, but it agrees fairly well with the measurements during the tip–sample contact.

Print publication: Issue 8 (27 February 2008)
Received 8 October 2007, in final form 24 December 2007
Published 4 February 2008

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