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KEY COMPARISON

Final report on EUROMET.T-K4 (EUROMET Project 820): Comparison of the realizations of the ITS-90 at the freezing points of Al (660.323 °C) and Ag (961.78 °C)

D Heyer et al 2008 Metrologia 45 03003   doi: 10.1088/0026-1394/45/1A/03003  Help


D Heyer1, U Noatsch1, E Tegeler1, M Anagnostou2, E Turzo-Andras3, I Antonsen4, V Augevicius5, J Bojkovski6, A Bronnum7, V Chimenti8, S Duris9, E Filipe10, S Gaita11, J Gray12, D Head12, E Grudniewicz13, J Ivarsson14, M Kalemci15, O Kerkhof16, I Lobo10, S Nemeth3, A Pokhodun17, J Ranostaj9, E Renaot18, P Rosenkranz19, M Smid20, P Steur21, A Steiner22, M Valin18, T Veliki23 and T Weckström24
1 Physikalisch-Technische Bundesanstalt (PTB), Germany
2 Hellenic Institute of Metrology (EIM), Greece
3 National Office of Measures (OMH), Hungary
4 National Standards Laboratory (Justervesenet), Norway
5 Temperature Standard Laboratory (VMT/PFI), Lithuania
6 Laboratory of Metrology and Quality (MIRS/FE-LMK), Slovenia
7 Teknologisk Institut, Denmark
8 Centro Español de Metrologia (CEM), Spain
9 Slovak Institute of Metrology (SMU), Slovakia
10 Instituto Português da Qualidade (IPQ), Portugal
11 Institut National de Metrologie (INM), Romania
12 National Physical Laboratory (NPL), UK
13 Central Office of Mesures (GUM), Poland
14 Swedish National Testing and Research Institute (SP), Sweden
15 Ulusal Metroloji Enstitsu (UME), Turkey
16 National Metrology Institute (NMi), The Netherlands
17 DI Mendeleyev Institute of Metrology, Russia
18 Institut National de Metrologie (LNE–INM/CNAM), France
19 Bundesamt für Eich- und Vermessungswesen (BEV), Austria
20 Czech Metrology Institute (CMI), Czech Republic
21 Istituto Nazionale di Ricerca Metrologica (INRiM), Italy
22 Federal Office of Metrology (METAS), Switzerland
23 University of Zagreb (FSB-LPM), Croatia
24 Centre for Metrology and Accreditation (Mikes), Finland

Abstract. The comparison EUROMET.T-K4 is the regional extension of CCT-K4: an intercomparison of the realisations of the freezing points of Al (660.323 °C) and Ag (961.78 °C). The intercomparison was organized in four loops with long stem standard platinum resistance thermometers (SPRTs) as travelling standards: One 25 Ω thermometer to be used only at the Al freezing point and two high temperature SPRTs to be used only at the Ag freezing point in each loop. Parallel to the measurements with thermometers the pilot and sub-pilots organized an internal intercomparison using an Ag fixed point cell.

Most HTSPRTs showed a strong drift which is mainly due to mechanical stress and poisoning of the sensor by impurities. This drift can partly be compensated by a correction applying Matthiessen's rule. An evaluation of the data taking into account both HTSPRTs in each loop, the linkage of the sub-pilots by measurements at the Ag freezing point and a possible compensation according to Matthiessens's rule allows to calculate the results of the participants also for the measurements at the Ag freezing point. European reference values (ERV) were calculated for measurements at the Al and Ag freezing points. The difference between these ERVs and the corresponding KCRVs of CCT-K4 is also given, which allows the linking of the different comparisons.

Main text. To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/.

The final report has been peer-reviewed and approved for publication by the CCT, according to the provisions of the CIPM Mutual Recognition Arrangement (MRA).

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